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Details
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Effect of the TEOS/Al(i-pro)(3) mol ratio in the composition on the crystal morphology of zeolites
Author |
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Kim, I. J.; Zhao, W.; Fan, X. O.; Chang, J. H.; Gauckler, L. J. |
Year |
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2010 |
Type
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Journal Article |
Journal |
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Journal of Ceramic Processing Research |
Volume |
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11 |
Issue |
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2 |
Pages |
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158-163 |
ISSN |
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1229-9162 |
Accession Numer |
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WOS:000277892400006 |
Abstract |
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The interest is focused on the control of crystal morphology of single phase zeolite nanocrystals from cube, LTA to octahedron, Faujasite by the mol ratio of TEOS /Al(i-pro)(3) in the mother solution, a Al(i-pro)(3) : 2.2 TEOS: 2.4-5.7 TMAOH: 0.3 NaOH : 200 H2O compositions. Well- controlled single nanocrystals of a high quality zeolite LTA with a size of 264 nm and sodalite with a size of 30-50 nm were synthesized by the compositions having a TEOS /Al(i-pro)(3) : 2.2 and 5.2, respectively. The synthesized crystals were characterized by scanning electron microscopy (SEM). high resolution transmission electron microscopy(HRTEM), X-ray powder diffraction(XRD), and dynamic light scattering (DLS). |
Notes |
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Times Cited: 0 |
URL |
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Access publication [Website]
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Record Number |
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736 |
Group
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nonmet |
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