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HREM observation of stacking sequences in bulk Bi-Sr-Ca-Cu-O superconductors and identification of phases by ED and EDX

Author   Heinrich, H.; Kostorz, G.; Heeb, B.; Muller, R.; Schweizer, T.; Gauckler, L.J.
Year   1993
Type   Journal Article
Journal   Ultramicroscopy
Volume   49
Issue   1-4
Pages   265-272
Date   1993/2
Custom 1   JA
Custom 2   SUPRA
Abstract   Melt-processed polycrystalline Bi2Sr2CaCu2O8+[delta] specimens contain a variety of phases. A systematic identification is presented of the different non-superconducting phases besides the grains of Bi2Sr2CaCu2Oy (2212) superconductors by HREM, ED and EDX. The Ca and Cu concentrations of the superconducting grains are reduced owing to the existence of several other phases in melt-processed specimens. The transformation of (2201) grains to (2212) grains upon heat treatment and different stacking sequences in (2212) grains are identified. [Author abstract; 13 Refs; In English]
URL  
Record Number   111
Group   nonmet

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